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Advanced Organic Synthesis

A Laboratory Manual

Edition:
1st
Author(s):
Dmitry V. Liskin, Penny Chaloner
ISBN:
9781482244960
Format:
Paperback
Publication Date:
November 24, 2015
Content Details:
107 pages
Language:
English

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$195.00

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  • About the Book

    Book Summary

    Laboratory experience equips students with techniques that are necessary for professional practice. Advanced Organic Synthesis: A Laboratory Manual focuses on a mechanistic background of key reactions in organic chemistry, gives insight into well-established trends, and introduces new developments in the field.

    The book features experiments performed by primary author Dmitry Liskin while he was a graduate student, providing a real-life quality to the experiments by using examples that have actually been conducted. It also includes recent experiments that have been published in peer-reviewed journals. The experiments are presented in a brief and simple manner, including bulleted lists of the required materials and equipment as well as step-by-step walkthroughs. Each experiment also carefully details safety issues and waste disposal methods.

    Emphasizing techniques and approaches used in more advanced labs, Advanced Organic Synthesis: A Laboratory Manual gives undergraduates the theoretical knowledge and practical experience they need to succeed at more advanced levels of research involving organic synthesis at the graduate or industrial level.

    Features

      • Provides undergraduates with the theoretical knowledge and practical background they need to succeed in graduate school or industrial fields
      • Focuses on a mechanistic background of key reactions in organic chemistry
      • Covers well-established trends as well as new developments in the field
      • Presents each experiment in a clear and concise manner, including safety issues and waste disposal
  • Contents

    Diastereoselective Reduction of Estrone
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Synthesis of 2,2-Dimethyl-4-pentene-1-amine
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Protection of 2,2-Dimethyl-4-pentene-1-amine
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Optimization of the Reaction Conditions for the Aminofluorination of N-(2,2-Dimethylpent-4-enyl)-2-toluenesulfonamide
    Equipment Required
    Materials Required
    Procedure
    References

    Asymmetric Robinson Annulation
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Formation of N-Benzylcinchonidinium Chloride from Cinchonidine
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure

    Chiral Resolution of BINOL (1,1’-bi-2-Naphthol) with N-Benzylcinchonidinium Chloride
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Transesterification of Phosphatidylcholine and FAME Quantification
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Green Chemistry: Solventless Sequential Aldol and Michael Reactions in the Synthesis of Kröhnke Pyridine
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Carbonyl Chemistry in a Multistep Synthesis
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Multistep Synthesis of a Bioactive Peptidomimetic
    Equipment Required
    Materials Required
    Stock Solutions
    Overall Reaction
    Procedure
    References

    Total Synthesis of a Natural Product: Caffeic Acid Phenethyl Ester (CAPE)
    Equipment Required
    Materials Required
    Overall Reaction
    Procedure
    References

    Appendix: Essential Laboratory Techniques
    Choosing Glassware
    Drying Glassware
    Purging with Inert Gas
    Setting a Pressure Release Valve
    Handling of Pyrophoric and Water-Sensitive Reagents
    Setting Up a Chromatography Column
    Pulling Spotters
    Spotting and Running a TLC Plate
    Dry Solvents and Reagents
    Setting Up an Apparatus